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and materials science.

Syntheses

Titanium ethoxide is prepared by treating titanium tetrachloride with ethanol in the presence of an amine:
:TiCl₄ + 4 EtOH + 4 Et₃N -> Ti(OEt)₄ + 4 Et₃NHClThe purity of titanium ethoxide is commonly assayed by proton NMR spectroscopy. Ti(OEt)₄ 1H NMR (90 MHz, chloroform-d, ppm): 4.36 (quartet, 8H, CH₂), 1.27 (triplet, 12H, CH₃).

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