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<p>in 1599 Galileo attempted the <a href="page.php?w=Quadrature_%28geometry%29">quadrature</a> of the cycloid (determining the area under the cycloid) with an unusually empirical approach that involved tracing both the generating circle and the resulting cycloid on sheet metal, cutting them out and weighing them.  He discovered the ratio was roughly 3:1, which is the true value, but he incorrectly concluded the ratio was an irrational fraction, which would have made quadrature impossible.  Around 1628, <a href="page.php?w=Gilles_de_Roberval">Gilles Persone de Roberval</a></p><p>
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